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400 MHz NMR Spectroscopy

Methods IPH, Müller

NMR spectroscopy Model: Bruker Avance DRX 400
Unit and Room: Pharmaceutical Chemistry, 02.050 A
Responsible: S. Ferlaino
Spectroscopy Further information: http://portal.uni-freiburg.de/magres/equipment/nmr_spektrometer/nmr1_pharmwiss.html

Short Description:

NMR spectrometer with autosampler including BBO (broad band observe) 5mm with Z-gradient (Standard) and TXI , 1.7 mm with Z-gradient (on request).

Picture of the Equipment

Bruker 400 MHz NMR Spectrometer
 

Available Experiments/Techniques:

Standard 1D, 2D techniques, Heteronuclear measurements, Selective experiments including all decoupling techniques and multipulse sequences 

Special Equipment:

Variable temperature unit (253-393 K) 

Measurements on the equipment are currently done by: Trained scientific service personal
 
Recent Publications, where this instrument was
important (citation):
Journal of Mass Spectrometry 2009, 44, 832-837.
PNAS 2009, 106, 8877-8882.
 
Typical problems that may be solved with this instrument: - Structural elucidation of biological compounds
- Quantitative determinations and following the reaction mechanism
- Elucidation of the reaction kinetics.

 

pdficon.gif 400 MHz NMR Spectroscopy (this page as a pdf file)

 

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