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Semipreparative HPLC

Methods IOC, Breit/Brückner/Plattner

Semipreparative HPLC Model: Knaur Well Chrom
Unit and Room: Org. Chem., R 07 016
Responsible: Dr. Richard Krieger
Chromatography Further information:  
Short Description:

Semipreparative HPLC with high pressure gradient pumps, manual/automatic injection valve, UV-detektion monochromatic, fraction collection valve, pc software for instrument control and data analysis and reporting (Eurochrom prep. version ca 5 years old)

 Picture of the Equipment

semipreparative HPLC
 
Available Experiments/Techniques:

-semiprep. separations of racemates using normal phase conditiones with monochromatic uv/vis detection,
- semiprep purifications using normal phase or reversed phase conditions of achiral compounds 

Special Equipment:

semipreparative columnes:
chiral Daicel AD-H, OD-H,
achiral: RP-18e, Eurosphere 100 C18 (reversed phase), Silica Si 100 normal phase
Measurements on the equipment are currently done by:

Trained scientific service personal

 
Recent Publications, where this instrument was
important (citation):

 

 
Typical problems that may be solved with this instrument:

-semipreparative separation of racemates,
-semipreparative separation of mixtures of isomers or complex mixtures at normal and reversed phase conditions with monochromatic uv/vis detection

 

pdficon.gif Semipreparative HPLC (this page as pdf file)
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