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Analytical HPLC 1

Methods IOC, Breit/Brückner/Plattner

Analytical HPLC 1 Model: Merck Hitachi LaChrom 2x
Unit and Room: Org. Chem., R 07 016
Responsible: Dr. Richard Krieger
Chromatography
Further information:  
Short Description:

Analytical HPLC with degasser, low pressure gradient pump, rheodyne manual injection, columne thermostat and UV-detection, computer, software for instrument control, data analysis and reporting (hsm 12 years old)

Picture of the Equipment

Analytical HPLC 1
 

Available Experiments/Techniques:

-ee-determination normal phase,
-quantification at spezific wavelength,
-separation of mixtures at analytical scale using monochromatic uv/vis detection

Special Equipment:

columnes:
chiral: analytical columnes normal phase conditions from Daicel (AD-H, OD-H, IA, IB, IC), one Pirkle Phase (Whelk O2), one Cyclodextrine phase,
chiral analytical columnes reversed phase conditions from Daicel: AD-3R, OD-R, OJ-R
achiral: rp selectB, rp 18,rp18e (reversed phase, Lichrosphere Merck, old columnes) , silica (normal phase Si60 Lichroshere Merck, nucleosil 100 Macherey Nagel, old columnes)

Measurements on the equipment are currently done by:

Trained scientific service personal

 

Recent Publications, where this instrument was
important (citation):

 

 

Typical problems that may be solved with this instrument:

-ee determination,
-elaboration and analysis of semiprep. separations of racemates,
-elaboration and analysis of semiprep. separations of complex mixtures of regio- and stereoisomers,
-separation of mixtures at analytical scale using monochromatic uv/vis detection
-quantifications at spezific wavelengths

 

pdficon.gif Analytical HPLC 1 (this page as pdf file)

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