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Size Exclusion Chromatography

Methods IMC, Mühlhaupt

Size Exclusion Chromatography Model: PSS Agilent 1200/1260 Series
Unit and Room: Inst.f.Makro.Mol.Chem., R.-1.010
Responsible: Marina Hagios, -1.009
SEC/GPC
Further information: http://portal.uni-freiburg.de/makro-chemie/zentrein/servicegroup/gpc

Short Description:

3 PSS/Agilent SEC Systems equipped with Refractive Index and UV detectors.
Solvents: Chloroform, THF and Water

Chloroform: 4 SDV columns 5µ (1000 A,10000 A,
100000 A, 1000000 A)

THF: 3 SDV columns 5µ (100 A,1000 A, 10000A)

Water: 3 Suprema columns 10µ (100A, 2x 3000A)

Organic Measurements at RT (~22,5°C)
Water Measurements at 40°C

 

Picture of the Equipment

Size Exclusion Chromatography
 

Available Experiments/Techniques:

Size exclusion chromatography of polymers in
chloroform ,THF or Water

Determination of molar mass distributions by
means of calibration with PS or other Calibrants

Special Equipment:

-

Measurements on the equipment are currently done by: Trained scientific service personal
 
Recent Publications, where this instrument was
important (citation):
Macromolecular Rapid Communications (2009), Volume 30, Issue 15, Pages 1323-1327
 
Typical problems that may be solved with this instrument: Determination of molar mass distributions, molar mass averages and polydispersity of polymer samples

 

pdficon.gif Size Exclusion Chromatography (this page as a pdf file)

 

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