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Electron Micro Probe Analyzer

Methods IGW, Müller-Sigmund

Electron Micro Probe Analyzer (EMPA) Model: Cameca SX 100
Unit and Room: Mineralogy, Lab Build., R. 01009
Responsible: Dr. Hiltrud Müller-Sigmund
Elemental Analysis by
X-ray emission spectra

Further information: http://www.minpet.uni-freiburg.de/sites/englisch/analytik/mikrosonde.html

Short Description:

The EMPA allows nominally non-destructive, quantitative analyses of elements with Z>3 in solids; polished and conductive sample surface required (limited range of samples sizes, including 40mm round, 1 inch round, 48x28mm, max. thickness ca. 1 cm)

Picture of the Equipment

Electron Micro Probe Analyzer (EMPA)
 

Available Experiments/Techniques:

- quantitative analyses
- element mapping
- concentration profiles
- (thin film and single particle analysis) 
 
Special Equipment:

30 kV electron gun, W-filament
Five vertical wavelength-dispersive spectrometers
Integrated Link (Oxford) nitrogen cooled ED-system (element range Na-U)
Optical microscope: reflected and transmitted light optics and polariser
Edwards Auto 306 sputter-coater for carbon coating

Measurements on the equipment are currently done by: Students after extensive training
Trained scientific service personal
 
Recent Publications, where this instrument was
important (citation):
Parat F. et al. 2010: Experimental constraints on ultrapotassic magmatism from the Bohemian Massif (durbachite series, Czech Republic). Contributions to Mineralogy and Petrology 159, 331-347.
 
Typical problems that may be solved with this instrument: element concentrations in solids, element distribution, thin film analysis

 

pdficon.gif Electron Micro Probe Analyzer (this page as a pdf file)

 

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