Differential Scanning Calorimeter
Methods IAAC, Krossing
| Differential Scanning Calorimeter | Model: | Setaram DSC 131 |
| Unit and Room: | Inorg. Chem. 3rd floor, R.341 | |
| Responsible: | Witali Beichel |
|
| Phase Transitions, Decomposition |
Further information: | Witali.Beichel@fmf.uni-freiburg.de |
| Short Description: Differential scanning calorimeter with a plate shaped DSC rod for determination of transition points and enthalpies in a wide temperature range (-150-700 °C) at different scanning rates. |
Picture of the Equipment
|
|
| Available Experiments/Techniques: Heating in the temperature range 25-700 °C, cooling from 25-(-150 °C) at different scanning rates (1-50 °C/min); use with different carrier gases; regulation of gas flow; aluminium, alumina and high pressure crucibles. |
||
| Special Equipment: Commercial licenses: Turbomole, Gaussian 03, Cosmotherm, Crystal 06 |
||
| Measurements on the equipment are currently done by: | Trained scientific service personal |
|
| Recent Publications, where this instrument was important (citation): |
Chem. Europ. J. 2009, 15, 1966-1976. J. Am. Chem. Soc. 2006, 128, 13427-13434. |
|
| Typical problems that may be solved with this instrument: | Determination of melting, crystallization, glass transition, decomposition point, dehydration, Cp, reaction enthalpies, transition enthalpies, reaction kinetics. | |
Differential Scanning Calorimeter (this page as a pdf file)