Single-crystal X-ray Diffraction
Methods IAAC, Hillebrecht
| Single-crystal X-ray Diffraction | Model: | STOE IPDS2 |
| Unit and Room: | Inorg. Chemistry, Chem. II, basement R. -142 | |
| Responsible: | Dr. M. Ade | |
| X-ray Diffraction | Further information: | http://portal.uni-freiburg.de/fkchemie/ Ausstattung/roentgenbeugung |
| Short Description: X-ray diffractometer for single crystal structure determination; 2-Circle Goniometer, 340 mm diameter imaging plate area detector with 2thetamax = 77°; variable detector distance (40-200 mm); Mo-Kalpha-radiation, X-ray wave guide and linear graphite monochromator |
Picture of the Equipment
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| Available Experiments/Techniques: single-crystal X-ray diffraction, automatic data collection, indexing and integration prcedures; absorption correction based on crystal shape data;reciprocal lattice viewing possibility for detection of superstructures, twins and modulated structures |
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Special Equipment: high temperature attachment for measurements from RT up to 1000 K |
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| Measurements on the equipment are currently done by: | Students after extensive training Trained scientific service personal |
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| Recent Publications, where this instrument was important (citation): |
J. Am. Chem. Soc. 2009, 131, 12172; 9; J. Solid State Chem. 182 (2009) 995-1002; Chem. Eur. J. 2008, 14, 7331; Angew. Chem. 2005, 118, 172. |
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| Typical problems that may be solved with this instrument: | single-crystal structure determination examination of twinned crystals, modulated and superstructures |
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Single-crystal X-ray Diffraction (this page as a pdf file)