X-ray powder diffraction (PSD)
Methods IAAC, Hillebrecht
| X-ray powder diffraction | Model: | STOE STAD PSD |
| Unit and Room: | Inorg. Chem. basement, Chemistry II, R -142 | |
| Responsible: | Dr. Thilo Ludwig | |
| X-ray Diffraction, PSD Detector |
Further information: | http://portal.uni-freiburg.de/fkchemie/ Ausstattung/roentgenbeugung |
| Short Description: X-ray powder diffractometer with Transmission/Debye-Scherrer goniometer, Mo-Kalpha-radiation, Ge(111)monochromator and linear position sensitive detector (PSD) |
Picture of the Equipment
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| Available Experiments/Techniques: Transmission measurement with flat specimen; Debye-Scherrer measurements with capillary specimens for air and moisture sensitive samples. |
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| Special Equipment High-temperature attachment for capillaries up to 1000 K available. |
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| Measurements on the equipment are currently done by: | Students after extensive training Trained scientific service personal |
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| Recent Publications, where this instrument was important (citation): |
Z. Anorg. Allg. Chem. 635 (2009) 653-659; J. Solid State Chem. 182 (2009) 538-546; Solid State Sciences 10 (2008) 291-302. |
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| Typical problems that may be solved with this instrument: | phase analysis; determination of cell parameters (indexing); Rietveld refinement; observation of temperature-dependet phase transitions | |
X-ray powder diffraction (PSD) (this page as a pdf file)